HRID234448

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2734389

4-(Trifluoromethyl)phenylboronic acid

C7H6BF3O2

HCID23445587

未命名化合物

PRODUCTS

生成物

结构：O=S(=O)(c1ccc(-c2ccc(C(F)(F)F)cc2)s1)n1cccc1

HCID22998451

未命名化合物

收率 75%

PROCEDURE

实验过程

N-{5-[4-(trifluoromethyl)phenyl]thiophene-2-sulfonyl}pyrrole was prepared in the same manner as described in Example 32C using 4-trifluoromethylbenzene boronic acid and N-(5-bromothiophene sulfonyl)pyrrole. Purification by column chromatography using 2% ethyl acetate/hexanes gave the pure sulfonamide as a white powder in 75% yield.

WORKUP

后处理

customPurification by column chromatography