HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(3,3-Diethyl-ureido)-benzenesulfonyl chloride → 3-Amino-5-chloro-1-[4-(N',N'-diethylureido)benzenesulfonyl]-1,3-dihydro-3-(2-methoxyphenyl)indol-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(3,3-Diethyl-ureido)-benzenesulfonyl chloride | HCID 2758245 | — |
| Reactant | 3-Amino-5-chloro-1,3-dihydro-3-(2-methoxyphenyl)indol-2-one | HCID 21925414 | — |
| Product | 3-Amino-5-chloro-1-[4-(N',N'-diethylureido)benzenesulfonyl]-1,3-dihydro-3-(2-methoxyphenyl)indol-2-one | HCID 19076408 | — |
Reaction Steps
This compound is prepared according to the procedure described in EXAMPLE 1 from 0.266 g of 3-amino-5-chloro-1,3-dihydro-3-(2-methoxyphenyl)indol-2-one and 0.280 g of 4-(N',N'-diethylureido)benzenesulfonyl chloride. The expected product is obtained after crystallization from a DCM/iso ether mixture. m=0.160 g. M.p.=214°-217° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05594023 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-0badf54af41047feb7099f6827422e14 |
| Source note | uspto-grants-1997_01 |