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HRID234522

反应详情

EQUATION

反应方程式

HRID 234522 的结构方程式

REACTANTS

反应物

2
结构：COc1cc([N+](=O)[O-])ccc1S(=O)(=O)Cl
HCID309458

2-Methoxy-4-nitrobenzenesulfonyl chloride

C7H6ClNO5S

结构：CCOc1ccc2c(c1)C(N)(c1ccccc1Cl)C(=O)N2
HCID19076387

未命名化合物

PRODUCTS

生成物

1
结构：CCOc1ccc2c(c1)C(N)(c1ccccc1Cl)C(=O)N2S(=O)(=O)c1ccc([N+](=O)[O-])cc1OC
HCID19076411

未命名化合物

PROCEDURE

实验过程

This compound is prepared according to the procedure described in EXAMPLE 16 from 3-amino-3-(2-chlorophenyl)-5-ethoxy-1,3-dihydroindol-2-one and 2-methoxy-4-nitrobenzenesulfonyl chloride. Crystallization from a DCM/iso ether mixture gives the expected product, which crystallizes with 0.25 mol of iso ether. M.p.=129°-132° C.

WORKUP

后处理

  1. customThis compound is prepared
  2. customCrystallization from a DCM/iso ether mixture