4-Methoxybenzoic Acid → HCID 178455401, compound

HRID 234559Notes

Reaction equation

HRID 234559 reaction equation
[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([OH:9])=[O:8])=[CH:5][CH:4]=1.[C:12]1([Si:18]2(CCCC)[CH2:23][CH2:22][CH:21]([CH:24]3[CH2:29][CH2:28][CH:27](O)[CH2:26][CH2:25]3)[CH2:20][CH2:19]2)C=C[CH:15]=[CH:14][CH:13]=1>>[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([O:9][C@H:27]2[CH2:26][CH2:25][C@H:24]([CH:21]3[CH2:20][CH2:19][SiH:18]([CH2:12][CH2:13][CH2:14][CH3:15])[CH2:23][CH2:22]3)[CH2:29][CH2:28]2)=[O:8])=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 74784-Methoxybenzoic AcidHCID 233548284-(4-Phenyl-4-n-butyl-4-silacyclohexyl)cyclohexanol

Product 1

HCID 178455401HCID 178455401, compound

Procedure

The general procedure of Example 31 was repeated using 4-methoxybenzoic acid and 4-(4-phenyl-4-n-butyl-4-silacyclohexyl)cyclohexanol, thereby obtaining the intended product.

Workup

  1. customobtaining the intended product

Sources & evidence

ORD record
ord-a20192c6c32248f69d94f52483450cb4
Source dataset
uspto-grants-1997_01
Patent number
US05595686

Reaction notes

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