4-Fluorobenzoic Acid → HCID 178494939, compound

HRID 234561Notes

Reaction equation

HRID 234561 reaction equation
[F:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][CH:3]=1.[CH3:11][O:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH:18]1[CH2:23][CH2:22][CH:21]([SiH:24]2[CH2:29][CH2:28][CH:27](O)[CH2:26][CH2:25]2)[CH2:20][CH2:19]1>>[F:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([O:8][C@H:27]2[CH2:28][CH2:29][Si@H:24]([CH:21]3[CH2:22][CH2:23][CH:18]([CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][O:12][CH3:11])[CH2:19][CH2:20]3)[CH2:25][CH2:26]2)=[O:7])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 99734-Fluorobenzoic AcidHCID 124012527HCID 124012527, compound

Product 1

HCID 178494939HCID 178494939, compound

Procedure

The general procedure of Example 31 was repeated using 4-fluorobenzoic acid and 4-(4-(5-methoxypentyl)cyclohexyl)-4-silacyclohexanol, thereby obtaining the intended product.

Workup

  1. customobtaining the intended product

Sources & evidence

ORD record
ord-99cdbbe063d74e66a77d355e8b5862e5
Source dataset
uspto-grants-1997_01
Patent number
US05595686

Reaction notes

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