4-(Trifluoromethoxy)benzoic acid → HCID 178442198, compound

HRID 234562Notes

Reaction equation

HRID 234562 reaction equation
[F:1][C:2]([F:14])([F:13])[O:3][C:4]1[CH:12]=[CH:11][C:7]([C:8]([OH:10])=[O:9])=[CH:6][CH:5]=1.[CH2:15]([CH:20]1[CH2:25][CH2:24][CH:23]([SiH:26]2[CH2:31][CH2:30][CH:29](O)[CH2:28][CH2:27]2)[CH2:22][CH2:21]1)[CH2:16][CH2:17][CH2:18][CH3:19]>>[F:1][C:2]([F:13])([F:14])[O:3][C:4]1[CH:12]=[CH:11][C:7]([C:8]([O:10][C@H:29]2[CH2:30][CH2:31][Si@H:26]([CH:23]3[CH2:22][CH2:21][CH:20]([CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])[CH2:25][CH2:24]3)[CH2:27][CH2:28]2)=[O:9])=[CH:6][CH:5]=1

Participants

3

Reactant 2

HCID 676134-(Trifluoromethoxy)benzoic acidHCID 1236855214-(4-n-Pentylcyclohexyl)-4-silacyclohexanol

Product 1

HCID 178442198HCID 178442198, compound

Procedure

The general procedure of Example 31 was repeated using 4-trifluoromethoxybenzoic acid and 4-(4-n-pentylcyclohexyl)-4-silacyclohexanol, thereby obtaining the intended product.

Workup

  1. customobtaining the intended product

Sources & evidence

ORD record
ord-5efa8dc105224ab6971254ee60ac5785
Source dataset
uspto-grants-1997_01
Patent number
US05595686

Reaction notes

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