HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphate → 2-Amino-5-tert-butyl-benzothiazole-6-thiol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphate | HCID 1061 | — |
| Reactant | D-1,4-Dithiothreitol | HCID 446094 | — |
| Reactant | 5-Tert-butyl-6-thiocyanato-benzothiazol-2-yl-amine | HCID 15473838 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Amino-5-tert-butyl-benzothiazole-6-thiol | HCID 22572893 | — |
Reaction Steps
The title compound was prepared according to General Method 14 using 5-tert-butyl-6-thiocyanato-benzothiazol-2-yl-amine (Example L-1; 8 g, 30 mmol), dithiothreitol (18.7 g, 121 mmol), EtOH (200 mL), and phosphate buffer (50 mL). MS (APCI): 239 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06852711B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-cbb2200b505743f89d88f8471e6e0c7a |
| Source note | uspto-grants-2005_02 |