HRID234622

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10912840

8-(2H-1,3-Benzodioxol-5-yl)-1,4-dioxaspiro[4.5]decan-8-ol

C15H18O5

PRODUCTS

生成物

HCID13855633

8-(2H-1,3-Benzodioxol-5-yl)-1,4-dioxaspiro[4.5]dec-7-ene

C15H16O4

收率 73%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

A solution of 8-(1,3-benzodioxol-5-yl)-1,4dioxaspiro[4.5]decan-8-ol in toluene was reacted as described in example 2 to give the product (73%, mp: 75°-76° C.). Calc'd for C15H16O4 : C, 69.22%; H, 6.20%. Found: C, 69.19%; H, 6.14%.