HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxaspiro[4.5]dec-7-ene, 8-(1,3-benzodioxol-5-yl)- → HCID 15232683, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxaspiro[4.5]dec-7-ene, 8-(1,3-benzodioxol-5-yl)- | HCID 13855633 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15232683 | HCID 15232683 | 91% |
Reaction Steps
A mixture of 8-(1,3-benzodioxol-5-yl)-1,4-dioxaspiro[4,5]dec-7-ene and 10% palladium on charcoal in ethanol was reacted as described in example 3 to give the product (91%, mp: 115°-116° C.). Calc'd for C15H18O4 : C, 68.69%; H, 6.92%. Found: C, 68.35%; H, 6.84%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05595993 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-30d0366bb7b9400ab158bbf016be8b83 |
| Source note | uspto-grants-1997_01 |