Acetonitrile → HCID 23355210, compound
Reaction equation
Cl.Cl[CH2:3][CH2:4][NH:5][C:6]1[C:15]2[C:10](=[CH:11][C:12]([Cl:16])=[CH:13][CH:14]=2)[N:9]=[CH:8][CH:7]=1.[C:17](#[N:19])[CH3:18]>>[Cl:16][C:12]1[CH:11]=[C:10]2[C:15]([C:6]([NH:5][CH2:4][CH2:3][N:19]3[CH2:8][CH2:7][CH:6]([CH3:15])[CH2:18][CH2:17]3)=[CH:7][CH:8]=[N:9]2)=[CH:14][CH:13]=1Participants
3
Procedure
2.72 g from 2.5 g of N-(2-chloroethyl)-7-chloro-4-quinolinamine hydrochloride; colourless crystals from acetonitrile, m.p.: 154°-156° C.
Sources & evidence
- ORD record
- ord-f08ac075553a42649039e546ebedfa2b
- Source dataset
- uspto-grants-1997_01
- Patent number
- US05596002
Reaction notes
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