HuagongsheHuagongshe Chemistry Print Report · For research reference only
6979-97-1 → Thymidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6979-97-1 | HCID 2724348 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Thymidine | HCID 5789 | 80% |
Reaction Steps
Crude 3',5'-di-O-acetylthymidine was dissolved in 20 ml methanol, and 0.075 gm sodium was added. After 8 hrs the reaction was quenched with Amberlite IR 120 resin, filtered and concentrated to yield beta-thymidine (2.4 gm, 80%). m.p. 181°-183° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05596087 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-4cc11fb97f7d47c7a671f334bcbab49a |
| Source note | uspto-grants-1997_01 |