HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Toluene-4-thiosulfonic acid S-(4,5-diamino-2-tert-butyl-phenyl) Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | toluene-4-thiosulfonic acid S-(4,5-bis-tert-butoxycarbonylamino-2-tert-butyl-phenyl)ester | HCID 69756247 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Toluene-4-thiosulfonic acid S-(4,5-diamino-2-tert-butyl-phenyl) Ester | HCID 54523728 | — |
Reaction Steps
The title compound was prepared as described in Example VV-1 from toluene-4-thiosulfonic acid S-(4,5-bis-tert-butoxycarbonylamino-2-tert-butyl-phenyl)ester (prepared in Example UU-2; 15 g, 28 mmol), CH2Cl2 (100 mL), and HCl gas. MS(APCI): 351 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06852711B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-3d976d0590c74beea9760d1b8cc11b3b |
| Source note | uspto-grants-2005_02 |