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HRID23493

反应详情

EQUATION

反应方程式

HRID 23493 的结构方程式

REACTANTS

反应物

3
结构：O=[N+]([O-])O
HCID944

Nitric Acid

HNO3

结构：O=S(=O)(O)O
HCID1118

Sulfuric acid

H2O4S

结构：Cc1ccc(C(C)(C)C)cc1
HCID7390

4-tert-Butyltoluene

C11H16

PRODUCTS

生成物

1
结构：Cc1ccc(C(C)(C)C)cc1[N+](=O)[O-]
HCID10954415

4-tert-butyl-1-methyl-2-nitrobenzene

C11H15NO2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

Nitration was performed as described in General Method 12 using tert-butyl-4-methylbenzene (25 g), concentrated H2SO4 (92 g), 70% HNO3 (82 g), and H2O (25 g). The crude product was purified via distillation under vacuum.

WORKUP

后处理

  1. distillationThe crude product was purified via distillation under vacuum