HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3,4-Dichlorophenyl)acetonitrile → 2,4-Diamino-5-(3,4-dichlorophenyl)-6-trifluoromethylpyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3,4-Dichlorophenyl)acetonitrile | HCID 76690 | — |
| Reactant | 2,4-Diamino-5-(2,3,5-trichlorophenyl)-6-trifluoromethylpyrimidine | HCID 11772723 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | 2,4-Diamino-5-(3,4-dichlorophenyl)-6-trifluoromethylpyrimidine | HCID 19705114 | — |
Reaction Steps
This compound was made in an analogous manner to the compound of Example 4, from 3,4-dichlorophenylacetonitrile (Aldrich) mp. 252°-254.5° C.: TLC (SiO2 ; methanol/chloroform, 1:9) Rf=0.38.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05597827 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-b044dd87b31c41408ffdc7279f95db09 |
| Source note | uspto-grants-1997_01 |