2,4-Diamino-5-(2,3-dichlorophenyl-4-nitrophenyl)pyrimidine → 2,4-Diamino-5-(2,3-dichloro-4-nitrophenyl)-6-methylpyrimidine

HRID 234944Notes

Reaction equation

HRID 234944 reaction equation
NC1N=C(N)C(C2C=CC([N+:15]([O-:17])=[O:16])=CC=2C2C=CC=C(Cl)C=2Cl)=CN=1.[NH2:26][C:27]1[N:32]=[C:31]([NH2:33])[C:30]([C:34]2[CH:39]=[C:38]([N+]([O-])=O)[CH:37]=[C:36]([Cl:43])[C:35]=2[Cl:44])=[C:29]([CH3:45])[N:28]=1>>[NH2:26][C:27]1[N:32]=[C:31]([NH2:33])[C:30]([C:34]2[CH:39]=[CH:38][C:37]([N+:15]([O-:17])=[O:16])=[C:36]([Cl:43])[C:35]=2[Cl:44])=[C:29]([CH3:45])[N:28]=1

Participants

3

Reactant 2

HCID 197050892,4-Diamino-5-(2,3-dichlorophenyl-4-nitrophenyl)pyrimidineHCID 197051082,4-Diamino-5(2,3-dichloro-5-nitrophenyl)-6-methylpyrimidine

Product 1

HCID 197050312,4-Diamino-5-(2,3-dichloro-4-nitrophenyl)-6-methylpyrimidine

Procedure

This compound was made from the compound of Example 15 in an analogous manner to the compound of Example 39, mp. 265° C. Also obtained from this reaction was 2,4-diamino-5(2,3-dichloro-5-nitrophenyl)-6-methyl pyrimidine.

Workup

  1. customAlso obtained from this reaction

Sources & evidence

ORD record
ord-67243549b7f54ea3a871a92e1717bd51
Source dataset
uspto-grants-1997_01
Patent number
US05597827

Reaction notes

Loading…