Potassium Iodide → HCID 19705076, compound

HRID 234965Notes

Reaction equation

[NH2:1][C:2]1[N:7]=[C:6]([NH2:8])[C:5]([C:9]2[CH:14]=[C:13]([N+]([O-])=O)[CH:12]=[CH:11][C:10]=2[Cl:18])=[C:4]([CH3:19])[N:3]=1.N([O-])=O.[Na+].[I-:24].[K+]>>[NH2:1][C:2]1[N:7]=[C:6]([NH2:8])[C:5]([C:9]2[CH:14]=[C:13]([I:24])[CH:12]=[CH:11][C:10]=2[Cl:18])=[C:4]([CH3:19])[N:3]=1

Participants

Reactant 3

HCID 4875Potassium Iodide

HCID 19705068HCID 19705068, compound

HCID 23668193Sodium Nitrite

Product 1

HCID 19705076HCID 19705076, compound

Procedure

This compound was prepared in a similar manner to the compound of Example 54 by reaction of the diazonium salt with potassium iodide, mp. 232°-234° C.

Sources & evidence

ORD record: ord-4bec4cbb99d04f7f9fc71db84d82d27d
Source dataset: uspto-grants-1997_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05597827

Reaction notes

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