Methanesulfonyl chloride → HCID 19705059, compound

HRID 234967Notes

Reaction equation

HRID 234967 reaction equation
[NH2:1][C:2]1[N:7]=[C:6]([NH2:8])[C:5]([C:9]2[CH:14]=[C:13]([N+:15]([O-])=O)[CH:12]=[CH:11][C:10]=2[Cl:18])=[C:4]([CH3:19])[N:3]=1.[CH3:20][S:21](Cl)(=[O:23])=[O:22]>N1C=CC=CC=1>[NH2:1][C:2]1[N:7]=[C:6]([NH2:8])[C:5]([C:9]2[CH:14]=[C:13]([NH:15][S:21]([CH3:20])(=[O:23])=[O:22])[CH:12]=[CH:11][C:10]=2[Cl:18])=[C:4]([CH3:19])[N:3]=1

Participants

4

Reactant 2

HCID 31297Methanesulfonyl chlorideHCID 19705068HCID 19705068, compound

Product 1

HCID 19705059HCID 19705059, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

This compound was prepared from 2,4-diamino-5-(2-chloro-5-aminophenyl)-6-methylpyrimidine from Example 54 by reaction with methanesulphonylchloride in pyridine, mp. 234°-240° C.

Sources & evidence

ORD record
ord-e381c0a2c02f4765bc9137f13629216c
Source dataset
uspto-grants-1997_01
Patent number
US05597827

Reaction notes

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