m-Chloroperbenzoic acid → 3,6-di(p-nitrostyryl)pyridazine-N-oxide

Participants

Reaction Steps

33 g of this nitro compound (K') is reacted, with 15g of m-chloroperbenzoic acid in halogen-containing solvent (such as 1,2-dichloroethane) to obtain 27 g of 3,6-di(p-nitrostyryl)pyridazine-N-oxide (L'). The nitro group in the N-oxide compound (L') is selectively reduced under a neutral or basic condition to obtain 20 g of vermilion crystals of 3,6-di(p-aminostyryl)pyridazine-N-oxide (M').

Provenance & Evidence