2-Diethylaminobenzyl bromide hydrobromide → 2-(2-Diethylaminobenzylmercapto)-1H-thieno[3,4-d]imidazole
Reaction equation
[SH:1][C:2]1[NH:3][C:4]2[C:5](=[CH:7][S:8][CH:9]=2)[N:6]=1.Br.[CH2:11]([N:13]([CH2:22][CH3:23])[C:14]1[CH:21]=[CH:20][CH:19]=[CH:18][C:15]=1[CH2:16]Br)[CH3:12]>>[CH2:22]([N:13]([CH2:11][CH3:12])[C:14]1[CH:21]=[CH:20][CH:19]=[CH:18][C:15]=1[CH2:16][S:1][C:2]1[NH:6][C:5]2=[CH:7][S:8][CH:9]=[C:4]2[N:3]=1)[CH3:23]Participants
3
Procedure
1.47 g of 2-mercaptothieno[3,4-d]imidazole are reacted with 3.05 g of 2-diethylaminobenzyl bromide hydrobromide, and the product is worked up in analogy to the procedure described in Example 1.
Sources & evidence
- ORD record
- ord-3246411e6e2443d7a4b325bc5003b578
- Source dataset
- uspto-grants-1989_10
- Patent number
- US04871734
Reaction notes
Loading…