3-[N-methyl-N-((naphth-1-yl)-eth-2-yl)-amino-prop-3-yl]-7,8-dimethoxy-1,3-dihydro-2H-3-benzazepin-2-one → HCID 19847410, compound

HRID 2350932Notes

Reaction equation

HRID 2350932 reaction equation
[CH3:1][N:2]([CH:15]([N:18]1[C:24](=O)[CH2:23][C:22]2[CH:26]=[C:27]([O:32][CH3:33])[C:28]([O:30][CH3:31])=[CH:29][C:21]=2[CH:20]=[CH:19]1)[CH2:16][CH3:17])[CH:3]([C:5]1[C:14]2[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=2)[CH:8]=[CH:7][CH:6]=1)[CH3:4].[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH3:1][N:2]([CH:15]([N:18]1[CH2:24][CH2:23][C:22]2[CH:26]=[C:27]([O:32][CH3:33])[C:28]([O:30][CH3:31])=[CH:29][C:21]=2[CH:20]=[CH:19]1)[CH2:16][CH3:17])[CH:3]([C:5]1[C:14]2[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=2)[CH:8]=[CH:7][CH:6]=1)[CH3:4]

Participants

3

Reactant 2

HCID 198474813-[N-methyl-N-((naphth-1-yl)-eth-2-yl)-amino-prop-3-yl]-7,8-dimethoxy-1,3-dihydro-2H-3-benzazepin-2-oneHCID 21226445Aluminium lithium hydride

Product 1

HCID 19847410HCID 19847410, compound

Procedure

Prepared from 3-[N-methyl-N-((naphth-1-yl)-eth-2-yl)-amino-prop-3-yl]-7,8-dimethoxy-1,3-dihydro-2H-3-benzazepin-2-one and lithium aluminium hydride analogously to Example 8.

Sources & evidence

ORD record
ord-188e33761995495f831d803ff0d5e922
Source dataset
uspto-grants-1989_10
Patent number
US04871735

Reaction notes

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