HCID 13592035, compound → 2-(3-Hydroxypropyl)-4,6,7-trimethyl-2H-1,3-benzoxathiol-5-ol

HRID 2350989Notes

Reaction equation

HRID 2350989 reaction equation
C(OC(CCC([O:10][C:11]1[C:12]([CH3:29])=[C:13]([CH3:28])[C:14]2[O:18][CH:17]([CH2:19][CH2:20][C:21](OCC)=[O:22])[S:16][C:15]=2[C:26]=1[CH3:27])=O)=O)C.C(OC1C(C)=C(C)C2OC(C)SC=2C=1C)(=O)C>>[OH:10][C:11]1[C:12]([CH3:29])=[C:13]([CH3:28])[C:14]2[O:18][CH:17]([CH2:19][CH2:20][CH2:21][OH:22])[S:16][C:15]=2[C:26]=1[CH3:27]

Participants

3

Reactant 2

HCID 13592035HCID 13592035, compoundHCID 14802163HCID 14802163, compound

Product 1

HCID 1275772-(3-Hydroxypropyl)-4,6,7-trimethyl-2H-1,3-benzoxathiol-5-ol

Procedure

Ethyl 3-[5-(3-ethoxycarbonylpropionyloxy)-4,6,7-trimethyl-1,3-benzoxathiole-2-yl)propionate (prepared as described in Example 32) was used in the same process as described in (1) above, to give the title compound, whose melting point, infrared absorption spectrum and mass spectrum were the same as those of the product described in (a) above.

Sources & evidence

ORD record
ord-cc5b225bed534097ab040a37af0f7b85
Source dataset
uspto-grants-1989_10
Patent number
US04871762

Reaction notes

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