HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 14802198, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 4,6,7-Trimethyl-2-propyl-2H-1,3-benzoxathiol-5-ol | HCID 127576 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 14802198 | HCID 14802198 | 95.6% |
Reaction Steps
A mixture of 1.6 g of 5-hydroxy-4,6,7-trimethyl-2-propyl-1,3-benzoxathiole (prepared as described in Example 42), 0.8 g of acetic anhydride and 10 ml of pyridine was reacted at room temperature for 15 hours and the reaction mixture was then treated and purified in the same manner as described in Example 4, to give 1.8 g of the title compound as a pale yellow oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04871762 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-588ab997fdb841ddbf053b428f52c33a |
| Source note | uspto-grants-1989_10 |