HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86743421, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Bromothiophenol | HCID 66049 | — |
| Reactant | HCID 15617524 | HCID 15617524 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86743421 | HCID 86743421 | — |
Reaction Steps
The compound of Example 14(a), 2-(7-bromoheptyl)benzoic acid (0.6 g., 2.01 mm), was reacted with 4-bromothiophenol (0.60 g., 3 mm), and triethylamine (1.12 ml, 8.05 mm) in DMF (35 ml) as in Example 14(b) to afford the desired product. This was further purified by flash chromatography over silica gel with ethyl acetate in hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04871771 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-84bde1d0d48d468da68e26a4a58dd244 |
| Source note | uspto-grants-1989_10 |