HCID 32237, compound → HCID 86743420, compound

HRID 2351076Notes

Reaction equation

[N:1]1([CH2:6][C:7]([C:9]2[CH:14]=[CH:13][C:12](OC)=[CH:11][CH:10]=2)=O)[CH:5]=[CH:4][N:3]=[CH:2]1.[CH2:17]([NH:24][OH:25])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[N:1]1([CH2:6][C:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[N+:24]([O-:25])[CH2:17][C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[CH:5]=[CH:4][N:3]=[CH:2]1

Participants

Reactant 2

HCID 32237HCID 32237, compound

HCID 2794173Benzylhydroxylamine

Product 1

HCID 86743420HCID 86743420, compound

Procedure

2-(1H-Imidazol-1-yl)-1-phenyl-N-(phenylmethyl)ethanimine N-oxide (2, R1 =R2 =C6H5, X=CH) Compound 2 (R1 =R2 =C6H5, X=CH) was prepared by the procedure described in Example 1, Method B, by reacting 2-(1H-imidazol-1-yl)acetophenone (1, R1 =C6H5, X=CH) with N-benzylhydroxylamine. Compound 2 (R1 =R2 =C6H5, X=CH) was obtained as a light yellow oil.

Workup

custom2-(1H-Imidazol-1-yl)-1-phenyl-N-(phenylmethyl)ethanimine N-oxide (2, R1 =R2 =C6H5, X=CH) Compound 2 (R1 =R2 =C6H5, X=CH) was prepared by the procedure

Sources & evidence

ORD record: ord-3ea05912f1f945ffa4baed88e0f0d95d
Source dataset: uspto-grants-1989_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04871862

Reaction notes

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