참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Rhodium | HCID 23948 | — |
| 반응물 | Phosphine, tris(phenylmethyl)- | HCID 82101 | — |
| 용매 | Texanol | HCID 6490 | — |
| 생성물 | Rhodium Tribenzylphosphine | HCID 86743422 | — |
반응 단계
A catalyst charge comprised of 31.25 mg of rhodium (as rhodium 2-ethylhexanoate) and varying amounts of tribenzylphosphine (as noted in Table 3) dissolved in 0.2 liter of Texanol® solvent was charged to the reactor system described above. The reactor was maintained at 125° C. and operated continuously for seven hours. The reaction was conducted according to the general procedure set forth above. Operating parameters and reaction results are set forth in Table 3.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04871878 |
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| 출처 데이터셋 | uspto-grants-1989_10 |
|---|
| ORD ID | ord-ba968caa234e46b0b608476ce3c94700 |
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| 출처 메모 | uspto-grants-1989_10 |
|---|