Bromine → HCID 54523503, compound

Participants

Reaction Conditions

Reaction Steps

0.53 g of N-(1,3-dimethyl-4-ethoxycarbonyl-5-pyrazolesulfonyl)-N'-(4,6-dimethyl-2-pyrimidinyl)-thiourea is suspended in 30 ml of methanol, followed by adding dropwise 0.21 g of bromine while stirring at 0° C. The suspension is stirred at the same temperature for 30 minutes and then at room temperature for 30 minutes. Then the precipitating crystals are filtered and washed with methanol. Recrystallization of the crystals from acetonitrile yields 0.26 g of the title compound as colorless crystals.

Provenance & Evidence