HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → Aniline, N-(2,2,2-trifluoroethyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | HCID 10993805 | HCID 10993805 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Aniline, N-(2,2,2-trifluoroethyl)- | HCID 9596 | 90.8% |
Reaction Steps
250 mg (0.573 mmol) of (2,2,2-trifluoroethyl)phenyliodonium trifluoromethanesulfonate, 107 mg (1.15 mmol) of aniline and 5 ml of methylene chloride were reacted and worked up in the same manner as described in Reference Example 4 to obtain 91.1 mg of N-(2,2,2-trifluoroethyl)aniline as an oily substance. Yield, 92%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04873027 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-5d456a4c84e6411aa1338919de3e5b1a |
| Source note | uspto-grants-1989_10 |