HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Ethylaniline → N-ethyl-N-(2,2,2-trifluoroethyl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Ethylaniline | HCID 7670 | — |
| Reactant | HCID 10993805 | HCID 10993805 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-ethyl-N-(2,2,2-trifluoroethyl)aniline | HCID 13510111 | 98% |
Reaction Steps
203 mg (0.465 mmol) of (2,2,2-trifluoroethyl)phenyliodonium trifluoromethanesulfonate, 113 mg (0.931 mmol) of N-ethylaniline and 5 ml of methylene chloride were treated and worked up in the same manner as described in Reference Example 4 to obtain 92.6 mg of N-ethyl-N-(2,2,2-trifluoroethyl)aniline as an oily substance. Yield, 98%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04873027 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-00303ec1727f4327b70951890f3853b8 |
| Source note | uspto-grants-1989_10 |