N,N-Dimethylaniline → N,N-dimethyl-N-phenyl-N-2,2,2-trifluoroethylammonium trifluoromethanesulfonate

Participants

Reaction Steps

61 mg (0.50 mmol) of N,N-dimethylaniline was added to a solution of 218 mg (0.50 mmol) of (2,2,2-trifluoroethyl)phenyliodonium trifluoromethanesulfonate in an argon atmosphere at room temperature, and the mixture was stirred for 30 minutes. After completion of the reaction, the reaction mixture was concentrated and purified by silica gel thin-layer chromatography to obtain 157 mg (89%) of N,N-dimethyl-N-phenyl-N-2,2,2-trifluoroethylammonium trifluoromethanesulfonate.

Provenance & Evidence