Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Rhodium | HCID 23948 | — |
| Edukt | Phosphine, tris(phenylmethyl)- | HCID 82101 | — |
| Lösungsmittel | Texanol | HCID 6490 | — |
| Produkt | Rhodium Tribenzylphosphine | HCID 86743422 | — |
Reaktionsschritte
A catalyst charge comprised of 31.25 mg of rhodium (as rhodium 2-ethylhexanoate) and varying amounts of tribenzylphosphine (as noted in Table 3) dissolved in 0.2 liter of Texanol® solvent was charged to the reactor system described above. The reactor was maintained at 125° C. and operated continuously for seven hours. The reaction was conducted according to the general procedure set forth above. Operating parameters and reaction results are set forth in Table 3.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US04873213 |
|---|
| Quelldatensatz | uspto-grants-1989_10 |
|---|
| ORD ID | ord-10c543711fbd4d2286fad605ff01ec96 |
|---|
| Quellennotiz | uspto-grants-1989_10 |
|---|