4-Aminobenzoic Acid → HCID 504661, compound

HRID 2351276Notes

Reaction equation

HRID 2351276 reaction equation
[NH2:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]([CH3:11])[C:3]=1[C:4]([OH:6])=[O:5].C1C(C(O)=O)=CC=C(N)C=1.Cl[C:23]([O:25][CH2:26][CH3:27])=O.ClC([O-])=O>>[CH2:26]([O:25][C:23]1[O:5][C:4](=[O:6])[C:3]2[C:7]([CH3:11])=[CH:8][CH:9]=[CH:10][C:2]=2[N:1]=1)[CH3:27]

Participants

5

Reactant 4

HCID 9784-Aminobenzoic AcidHCID 10928Ethyl chloroformateHCID 1512106-Methylanthranilic acidHCID 21226386Carbonochloridate

Product 1

HCID 504661HCID 504661, compound

Procedure

By following the procedure of Part A, but replacing 2-amino-6-methyl benzoic acid with the appropriate aminobenzoic acid prepared in Preparation I, and/or replacing ethyl chloroformate with the appropriate chloroformate prepared in Preparation II, the following compounds of Formula (1) are prepared:

Workup

  1. customprepared in Preparation I

Sources & evidence

ORD record
ord-cd51a4ed58254262b5510386ceeb2342
Source dataset
uspto-grants-1989_10
Patent number
US04873232

Reaction notes

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