HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53652916, compound → HCID 15703648, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53652916 | HCID 53652916 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15703648 | HCID 15703648 | 87.5% |
Reaction Steps
A solution of 2-ethoxycarbonylamino-6-propenylbenzoic acid (220 mg) in ethanol was hydrogenated at 50 psi hydrogen over 10% palladium on charcoal. After 3 hours, the catalyst was filtered through Celite and the filtrate evaporated to give an oily solid (194 mg). IR νmax =1680-1740 (br), 2500-3200 (br).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04873232 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-9149b0cbbccf4902a4763ff0093c9a32 |
| Source note | uspto-grants-1989_10 |