HCID 14209990, compound → 2-[2-[(Diethylamino)methyl]piperidin-1-yl]ethanamine

HRID 2351383Notes

Reaction equation

HRID 2351383 reaction equation
[N:1]1([CH2:6][CH:7]2[CH2:12][CH2:11][CH2:10][CH2:9][N:8]2[CH2:13][C:14]#[N:15])[CH2:5][CH2:4][CH2:3][CH2:2]1.N1(CC2CCCCN2CCN)CCCC1>>[CH2:2]([N:1]([CH2:6][CH:7]1[CH2:12][CH2:11][CH2:10][CH2:9][N:8]1[CH2:13][CH2:14][NH2:15])[CH2:5][CH3:4])[CH3:3]

Participants

3

Reactant 2

HCID 14209990HCID 14209990, compoundHCID 14210016HCID 14210016, compound

Product 1

HCID 142100002-[2-[(Diethylamino)methyl]piperidin-1-yl]ethanamine

Procedure

from 2-[2-[(pyrrolidin-1-yl)methyl]-piperidin-1-yl]acetonitrile in a yield of 64% of theory, 2-[2-[(pyrrolidin-1-yl)methyl]-piperidin-1-yl]ethanamine, B.p.20 mm Hg 156°-158° C.;

Sources & evidence

ORD record
ord-4576a10014004a32b58163bc23d89e1f
Source dataset
uspto-grants-1989_10
Patent number
US04873236

Reaction notes

Loading…