HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropyl Ether → HCID 14210073, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | 5-chlorocarbonyl-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 13276745 | — |
| Reactant | 2-[(Dimethylamino)methyl]-1-piperidinepropanamine | HCID 14210003 | — |
| Product | HCID 14210073 | HCID 14210073 | 80% |
Reaction Steps
Prepared analogously to Example 2 from 5-(chlorocarbonyl)-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one and 3-[2-[(dimethylamino)methy]-piperidin-1-yl]propanamine in a yield of 80% of theory. Colourless crystals, m.p. 131°-133° C. (diisopropyl ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04873236 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-b585b47afdc2454ab3d3119cb6ed19e5 |
| Source note | uspto-grants-1989_10 |