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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2351396Generated: November 1, 2026

11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one → HCID 14210082, compound

https://huagongshe.com/reaction/2351396

Reaction equation

Participants

RoleNameHCIDCharge
Reactant11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-oneHCID 11043962—
ReactantHCID 19846036HCID 19846036—
SolventAcetonitrileHCID 6342—
ProductHCID 14210082HCID 1421008267%

Reaction Steps

Prepared analogously to Example 2 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 2-[3-[(diethylamino)methyl]-morpholin-4-yl]ethanamine in a yield of 67% of theory. Colourless crystals, m.p. 150°-151° C. (acetonitrile).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04873236
Source datasetuspto-grants-1989_10
ORD IDord-421e400dbbbd4a5da0e08d12d02c0988
Source noteuspto-grants-1989_10