HuagongsheHuagongshe Chemistry Print Report · For research reference only
11-(chlorocarbonyl)-6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepin-5-one → HCID 14210084, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 11-(chlorocarbonyl)-6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepin-5-one | HCID 14209983 | — |
| Reactant | 2-[2-[(Diethylamino)methyl]piperidin-1-yl]ethanamine | HCID 14210000 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 14210084 | HCID 14210084 | 52% |
Reaction Steps
Prepared analogously to Example 2 from 11-(chlorocarbony)-6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepin-5-one and 2-[2-[(diethylamino)methyl]-piperidin-1-yl]ethanamine in a yield of 52% of theory. Colourless crystals, m.p. 146°-147.5° C. (acetonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04873236 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-9674bbf76f0342ee8407f4adccf62b1d |
| Source note | uspto-grants-1989_10 |