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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2351409Generated: November 1, 2026

11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one → HCID 14210058, compound

https://huagongshe.com/reaction/2351409

Reaction equation

Participants

RoleNameHCIDCharge
Reactant11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-oneHCID 11043962—
ReactantHCID 19846058HCID 19846058—
SolventEthyl AcetateHCID 8857—
ProductHCID 14210058HCID 1421005810%

Reaction Steps

Prepared analogously to Example 2 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 2-[4-[2-(diethylamino)ethyl]-piperidin-1-yl]ethanamine in a yield of 10% of theory. Colourless crystals, m.p. 170°-172° C. (ethyl acetate).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04873236
Source datasetuspto-grants-1989_10
ORD IDord-0dc1ef0cd48f49c9b4d5e3ac246600fd
Source noteuspto-grants-1989_10