Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2351410Generated: November 2, 2026

11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one → HCID 14210059, compound

https://huagongshe.com/reaction/2351410

Reaction equation

Participants

RoleNameHCIDCharge
Reactant11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-oneHCID 11043962—
ReactantHCID 19845952HCID 19845952—
SolventEthyl AcetateHCID 8857—
ProductHCID 14210059HCID 1421005992%

Reaction Steps

Prepared analogously to Example 2 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 2[4-[3-(diethylamino)propyl]-piperidin-1-yl]ethanamine in yield of 92% of theory. Colourless crystals, m.p. 165°-166° C. (ethyl acetate).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04873236
Source datasetuspto-grants-1989_10
ORD IDord-c07841c26b6e4c9182f6ae267b5bea82
Source noteuspto-grants-1989_10