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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2351415Generated: November 2, 2026

11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one → HCID 14210064, compound

https://huagongshe.com/reaction/2351415

Reaction equation

Participants

RoleNameHCIDCharge
Reactant11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-oneHCID 11043962—
ReactantHCID 14210020HCID 14210020—
SolventAcetonitrileHCID 6342—
ProductHCID 14210064HCID 1421006448%

Reaction Steps

Prepared analogously to Example 46 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 2-[3-[(dipropylamino)methyl]-piperidin-1-yl]ethanamine in a yield of 48% of theory. Colourless crystals, m.p. 153°-155° C. (acetonitrile).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04873236
Source datasetuspto-grants-1989_10
ORD IDord-6efe6f987fa441a9bfdc9505e35b09d6
Source noteuspto-grants-1989_10