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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2351416Generated: November 3, 2026

11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one → HCID 14210065, compound

https://huagongshe.com/reaction/2351416

Reaction equation

Participants

RoleNameHCIDCharge
Reactant11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-oneHCID 11043962—
ReactantHCID 14210021HCID 14210021—
SolventAcetonitrileHCID 6342—
ProductHCID 14210065HCID 1421006569%

Reaction Steps

Prepared analogously to Example 46 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 2[3-[(hexahydro-1H-azepin-1-yl)methyl]-piperidin-1-yl]ethanamine in a yield of 69% of theory. Colourless crystals, m.p. 135°-137° C. (acetonitrile).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04873236
Source datasetuspto-grants-1989_10
ORD IDord-32234c48f44f48ea8948a76bf60d2a57
Source noteuspto-grants-1989_10