HuagongsheHuagongshe Chemistry Print Report · For research reference only
11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one → HCID 19846024, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one | HCID 11043962 | — |
| Reactant | HCID 19846041 | HCID 19846041 | — |
| Reactant | Diisopropylether ethyl acetate | HCID 22281796 | — |
| Product | HCID 19846024 | HCID 19846024 | 19% |
Reaction Steps
Prepared analogously to Example 2 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 2-[3-[[(cyclohexyl)methylamino]methyl]-pyrrolidin-1-yl]ethanamine in a yield of 19% of theory. Colourless crystals, m.p. 166°-167° C. (ethyl acetate/methanol 1/1 v/v).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04873236 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-1881be9ff0de4fafba2d1b2ce9654704 |
| Source note | uspto-grants-1989_10 |