HuagongsheHuagongshe Chemistry Print Report · For research reference only
9-Chloro-11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one → HCID 54444081, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 9-Chloro-11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one | HCID 14209976 | — |
| Reactant | HCID 19846005 | HCID 19846005 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 54444081 | HCID 54444081 | 10% |
Reaction Steps
Prepared analogously to Example 1 from 9-chloro-11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 2-[4-[3-(piperidin-l-yl)propyl]-piperidin-l-yl]ethanamine in a yield of 10% of theory. Colourless crystals, m.p. 176°-177° C. (acetonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04873236 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-c75394adea644babab3bca798b11bcf1 |
| Source note | uspto-grants-1989_10 |