Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2351442Generated: November 3, 2026

11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one → HCID 54174153, compound

https://huagongshe.com/reaction/2351442

Reaction equation

Participants

RoleNameHCIDCharge
Reactant11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-oneHCID 11043962—
ReactantHCID 19846023HCID 19846023—
SolventAcetonitrileHCID 6342—
ProductHCID 54174153HCID 5417415330%

Reaction Steps

Prepared analogously to Example 2 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 2-[2-[(morpholin-4-yl)methyl]-piperidin-l-yl]ethanamine in a yield of 30% of theory. Colourless crystals, m.p. 167° C. (acetonitrile using fuller's earth).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04873236
Source datasetuspto-grants-1989_10
ORD IDord-f484de9484834092b75d7ad610ecf5ff
Source noteuspto-grants-1989_10