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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2351443Generated: November 3, 2026

11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one → HCID 19845931, compound

https://huagongshe.com/reaction/2351443

Reaction equation

Participants

RoleNameHCIDCharge
Reactant11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-oneHCID 11043962—
ReactantHCID 19845993HCID 19845993—
SolventAcetonitrileHCID 6342—
ProductHCID 19845931HCID 1984593136%

Reaction Steps

Prepared analogously to Example 2 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 2-[2-[4-(piperidin-l-yl)butyl]-piperidin-l-yl]ethanamine in a yield of 36% of theory. Colourless crystals, m.p. 154°-155° C. (acetonitrile).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04873236
Source datasetuspto-grants-1989_10
ORD IDord-50748a594ce044769db3f6fbdf367193
Source noteuspto-grants-1989_10