Benzo(B)Thiophene → HCID 19846308, compound

HRID 2351463Notes

Reaction equation

HRID 2351463 reaction equation
[OH:1][N:2]([CH:6](C1SC2C=CC(CC(C)C)=CC=2C=1)[CH3:7])[C:3]([NH2:5])=[O:4].[S:21]1[C:25]2[CH:26]=[CH:27][CH:28]=[CH:29][C:24]=2[CH:23]=[CH:22]1>>[OH:1][N:2]([CH:6]([C:23]1[C:24]2[CH:29]=[C:28]([CH2:23][CH:24]([CH3:29])[CH3:25])[CH:27]=[CH:26][C:25]=2[S:21][CH:22]=1)[CH3:7])[C:3]([NH2:5])=[O:4]

Participants

3

Reactant 2

HCID 7221Benzo(B)ThiopheneHCID 19846333HCID 19846333, compound

Product 1

HCID 19846308HCID 19846308, compound

Procedure

N-hydroxy-N-[1-(5-(2,2-dimethylethyl)benzo[b]thien-2-yl)-ethyl]urea. The desired compound was prepared according to the method of example 2, except using the material prepared as in step c, above, instead of benzothiophene. (R1 =NH2, A=CHCH3, X=S[2-isomer], Y=5-(CH3)3C).

Workup

  1. customthe material prepared as in step c

Sources & evidence

ORD record
ord-527a2e6ccd4b49a59b918032d29d5c6a
Source dataset
uspto-grants-1989_10
Patent number
US04873259

Reaction notes

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