HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 15613917, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 3-Acetamidophenyl acetate | HCID 85287 | — |
| Reactant | 1-(4-Nitrophenoxy)propan-2-one | HCID 308507 | — |
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 15613917 | HCID 15613917 | 30.6% |
Reaction Steps
A procedure similar to that described in Preparation 1 was repeated, except that 10 g of 2-hydroxy-4,6-dimethylacetophenone, 12 g of 4-nitrophenoxyacetone, 6 ml of pyrrolidine, 3 g of p-toluenesulfonic acid monohydrate and 200 ml of benzene were reacted, to afford 6.36 g of the title compound, colored a pale yellow and melting at 86°-88.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04873255 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-286c41e9a45844faa3b10dece0e02067 |
| Source note | uspto-grants-1989_10 |