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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2351533Generated: November 1, 2026

Methanol → HCID 15671147, compound

https://huagongshe.com/reaction/2351533

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantHCID 15613920HCID 15613920—
CatalystPalladiumHCID 23938—
SolventBenzeneHCID 241—
ProductHCID 15671147HCID 1567114779.4%

Reaction Steps

Following a procedure similar to that described in Preparation 4, 10 g of methyl 2-methyl-2-(4-nitrophenoxymethyl)-4-oxochroman-6-carboxylate (prepared as described in Preparation 43) were hydrogenated, using 2 g of 10% w/w palladium-on-carbon, 100 ml of methanol and 200 ml of benzene, to afford 7.3 g of the title compound as a pale yellow oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04873255
Source datasetuspto-grants-1989_10
ORD IDord-8145934da7204527b5b1b88475b2366a
Source noteuspto-grants-1989_10