HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 15671147, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 15613920 | HCID 15613920 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 15671147 | HCID 15671147 | 79.4% |
Reaction Steps
Following a procedure similar to that described in Preparation 4, 10 g of methyl 2-methyl-2-(4-nitrophenoxymethyl)-4-oxochroman-6-carboxylate (prepared as described in Preparation 43) were hydrogenated, using 2 g of 10% w/w palladium-on-carbon, 100 ml of methanol and 200 ml of benzene, to afford 7.3 g of the title compound as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04873255 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-8145934da7204527b5b1b88475b2366a |
| Source note | uspto-grants-1989_10 |