Propylene Glycol → HCID 88506966, compound
Reaction equation
[CH:1]([CH:13]1[CH2:18][C:17](=[O:19])[O:16][C:14]1=[O:15])=[CH:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH2:20]([OH:24])[CH:21]([OH:23])[CH3:22]>>[CH:1]([CH:13]1[CH2:18][C:17](=[O:19])[O:16][C:14]1=[O:15])=[CH:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH2:20]([OH:24])[CH:21]([OH:23])[CH3:22]Participants
3
Conditions
- Temperature
- 130 °C
Procedure
A mixture of 1.2 mol of dodecenylsuccinic anhydride, 0.9 mol of propylene glycol and 40% by weight heavy aromatic naphtha was heated at 130° C. in a 1 L 3-necked, round bottomed flask equipped with a condenser and a mechanical stirrer for 6.5 hours.
Workup
- customround bottomed flask equipped with a condenser and a mechanical stirrer for 6.5 hours
Sources & evidence
- ORD record
- ord-3a196866b45c4c1ba8de88be414c6b5b
- Source dataset
- uspto-grants-1989_10
- Patent number
- US04874395
Reaction notes
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