HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 54199707, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | (2-Methyl-3-nitrophenyl)(naphthalen-1-yl)methanone | HCID 14535917 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54199707 | HCID 54199707 | — |
Reaction Steps
Following a procedure similar to that described in Preparation 2A above, 57 g (0.195 mole) of 2-methyl-3(1-naphthylcarbonyl)nitrobenzene and 103 ml (0.784 mole) of DMF dimethyl acetal in 300 ml of DMF was heated under reflux for seventeen hours and then taken to dryness to give 2-(2-dimethylaminoethenyl)-3-(1-naphthylcarbonyl)nitrobenzene as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04874761 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-11348116657347faa21ff6a726f77e43 |
| Source note | uspto-grants-1989_10 |