HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 57111376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Potassium cyanate | HCID 11378442 | — |
| Reactant | HCID 57120331 | HCID 57120331 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 57111376 | HCID 57111376 | 87.1% |
Reaction Steps
10 g of 4-tetrafluoroethoxyaniline, prepared as in Example 1, in 40 ml of water, and 10 ml of 1:1 HCl, were reacted with 3.9 g of potassium cyanate. The mixture was stirred for 30 minutes and the formed solid was filtered out, rinsed with cool water, and dried to give 10.5 g of the desired compound, having a melting point of 167°-168° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04874786 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-cc37b8eed65d4e128faac90e168f2d02 |
| Source note | uspto-grants-1989_10 |